Things You'll Need
Instructions
Superheat the alloy as you would in the hardening process to around 350 degrees Fahrenheit, depending on the desired temper. You must use a heating source you can heat continually, without fluctuations in heat for 24 hours.
Heat soak the alloy. This is the primary difference between typical tempering, hardening and precipitation heat-treating. Heat-soaking the alloy means to leave it at the superheated temperature for 9 to 24 hours depending on the specified temper and alloy you're working with.
Cool the alloy to room temperature very gradually. To ensure gradual cooling, you may have to insulate the alloy from exposure to cold air. You can sometimes use an insulating material such as sand. The alloy can be immersed in superheated sand, so the insulating sand cools around the alloy, helping to moderate the drop in temperature.