Things You'll Need
Instructions
Mix one part nitric acid with three parts hydrochloric acid. This will produce aqua regia, which releases free chlorine that will dissolve the gold. As this reaction gives off noxious fumes, this should be done in a vented fume hood or in an area that is safe for such a reaction.
Add the gold-bearing material and allow it to dissolve. Some stirring may be required to speed the process along. The reaction gives off some heat, so allow it to cool before proceeding.
Filter out non-gold-bearing solids. Once the gold is dissolved, the remaining solids should be filtered. It may be worthwhile to save the solids, depending on what they consist of. Some scrap jewelry may contain silver that will have formed a solid (silver chloride) while the gold dissolved.
Add urea to the filtrate. The filtrate is the solution that remains after filtering. Urea can be found at many gardening stores in the fertilizer section. The urea eliminates the nitric acid from the filtrate. Add until the reaction stops fizzing. Appropriate ventilation is still required.
Precipitate the gold from the filtrate by adding ferrous sulfate. It should be added slowly. Precipitation will cause the solution to turn cloudy as the gold solidifies. Continue to add the ferrous sulfate until the filtrate starts to give of a sulfide (rotten egg) smell.
Filter the precipitated gold from the solution. Rinse the gold with water through the same filter to remove any trace chemicals. The remaining 24K gold precipitate can be dealt with as desired. Most often it will now be melted and cast into a desired form.