Things You'll Need
Instructions
Reduce the size of the specimen by cutting or breaking off excess matrix. Be very careful not to break through to the fossil specimen.
Prepare a bath of a weak acid such as acetic acid (vinegar), used straight and poured into a plastic bucket or tub. Muriatic acid, available at hardware and pool-supply stores, may be used instead of acetic acid; dilute this stronger acid heavily. To dilute, fill a plastic bucket or tub with one to two gallons of fresh water. Pour a small amount of muriatic acid---less than a cup---into the water. Do not allow the acid to splash on your skin or clothes.
Immerse the fossil specimen in the acid solution. The limestone will begin to bubble and fizz as it reacts with the acid. Use a pair of rubber dishwashing gloves to remove the specimens from the acid bath occasionally. Rinse the specimens with fresh water to check progress. When the limestone matrix has been dissolved, clean off any remaining debris with a soft-bristle brush and rinse the specimens thoroughly. Set the fossils in a safe place to dry.
Neutralize the remaining acid by adding baking soda until the mixture no longer fizzes. At that point, the solution is safe to pour down the drain. Rinse the sink and bucket well and flush completely with fresh water.