Things You'll Need
Instructions
Prepare your testing solutions and place them into testing bottles. One bottle will contain straight nitric acid, and in the second bottle you will put the aqua regia. Mix the aqua regia in the graduated cylinder and then carefully pour it into a testing bottle. Aqua regia is made by mixing one part nitric acid to three parts hydrochloric acid.
Scratch your samples, one at a time, across the testing stone to leave a mineral streak.
Pipette a small amount of nitric acid onto the rock streak. Optionally, you may also put acid directly on your sample.
Observe the color the acid turns when it reacts to the rock streak. If gold is present in more than 14 karat purity, there will be no reaction. If gold is present in 12 karat concentration, the sample will turn light brown. If 10 karat gold is present, the sample will turn dark brown. A pinkish cream color indicates a low concentration of gold. Blue indicates copper.
If the sample did not react, follow this second step to determine if there is gold present in a higher purity. On the opposite side of the testing stone, rub the rock across to leave a streak. Start with the 14K gold wire. Streak the wire across the plate beside the gold sample. Make sure the lines do not intersect.
Apply aqua regia to both streaks. The aqua regia will react---bubble and fizz---if it contacts gold. The acid will turn the same color when the purity of the ore sample matches the test wire. Aqua regia dissolves gold, so do not put it directly on your sample.
Repeat with higher-karat wire, if necessary, until the purity is determined.