Things You'll Need
Instructions
Place the glassware into the autoclave. Sterilize the glass and allow it to cool inside the autoclave. Fill the round-bottomed flask with water. Put the rubber stopper in the hole and place the apparatus on the ring stand over the Bunsen burner.
Attach the rubber tubes to the condenser and insert the condenser into the flask and place the volumetric flask under the condenser spout. Connect a tube to the faucet and place the other tube into the sink.
Turn on the gas feed to the Bunsen burner and light it with the gas lighter. Turn on the faucet and boil the flask until all the water collects in the volumetric flask. Cover the volumetric flask with parafilm to prevent contamination.